Low Activity of Regenerated Carbon and Fine Particle Issues at a Gold Mine in Victoria, Australia

Low Activity of Regenerated Carbon and Fine Particle Issues at a Gold Mine in Victoria, Australia

Introduction

With over 50 years of experience in the Activated Carbon Manufacturing Industry, Haycarb focuses on sustainable practices and provides high-performance activated carbon products that meet the rigorous demands of modern gold extraction processes. In addition to our advanced manufacturing techniques and quality control systems, our experienced multidisciplinary technical teams comprising of Chemists, Process Engineers and Metallurgists offer a wide range of services including tests and assays on Activated Carbon from our fully equipped laboratories together with the following suite of technical services for effective carbon selection and management.

With over 50 years of experience in the Activated Carbon Manufacturing Industry, Haycarb focuses on sustainable practices and provides high-performance activated carbon products that meet the rigorous demands of modern gold extraction processes. In addition to our advanced manufacturing techniques and quality control systems, our experienced multidisciplinary technical teams comprising of Chemists, Process Engineers and Metallurgists offer a wide range of services including tests and assays on Activated Carbon from our fully equipped laboratories together with the following suite of technical services for effective carbon selection and management.

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Routine

Testing

Evaluating the condition of plant carbons, regeneration efficiency and process carbon management.

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Technical

Troubleshooting

Identifying and resolving issues related to activated carbon systems.

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Activated Carbon Plant

Audits

Conducting comprehensive evaluations of activated carbon plants to ensure optimal performance.

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Plant Operator

Training

Providing specialized training for plant operators on effective carbon management.

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Routine Testing

Evaluating the condition of plant carbons, regeneration efficiency and process carbon management.

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Technical Troubleshooting

Identifying and resolving issues related to activated carbon systems.

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Activated Carbon Plant Audits

Conducting comprehensive evaluations of activated carbon plants to ensure optimal performance.

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Plant Operator Training

Providing specialized training for plant operators on effective carbon management.

The following is an example of how our Technical trouble shooting and mine audit process of a Gold Mine in Victoria, Australia that faced with 2 main issues: low activity of regenerated carbon and unexpectedly fine particle distribution, was assisted by our team to identify the root cause and recommend solutions that overcame the problem successfully.

Upon brief investigation by our engineers, it was found that the main cause for operational inefficiencies and carbon attrition was the impaired function of the screw feeder in the regenerated kiln.

Problem Identification

Problem Identification

Activated Carbon Activity

The sample of regenerated carbon showed an activity level of just 59.7%, which is significantly lower than with new activated carbon. This indicates ineffective regeneration, adversely affecting the overall efficiency of gold recovery. Ideally, the activity of regenerated carbon should fall within the optimum range of 85% to 95%.

Root Causes
Root Causes
Contaminated Water Used for Quenching

The low activity observed in regenerated carbon is often not due to the regeneration process itself, but rather the quality of water used for Quenching. If the quench tank water is of poor quality (e.g. using process water with a higher percentage of contaminants), the regenerated carbon may adsorb contaminants at this stage, including both organic and inorganic substances.

As evidenced by ICP analysis, the quench water sample showed higher concentrations of inorganic contaminants. This significantly reduces the carbon’s activity, affecting its kinetic properties, gold adsorption capacity, and overall recovery rates. However, this issue does not occur in all gold processing operations.

Regeneration Issue

In this process, froth flotation utilizes organic reagents to recover gold concentrate. However, these reagents often carry over into the CIL process, contaminating the activated carbon and diminishing its gold adsorption efficiency. This indicates that the activated carbon regeneration process was flawed.

In this case, regeneration must be performed under more stringent conditions and at higher temperatures than usual because some reagents, particularly Potassium Amyl Xanthate (an organosulfur compound), bind very strongly to the carbon pores.

Contaminated Water Used for Quenching

The low activity observed in regenerated carbon is often not due to the regeneration process itself, but rather the quality of water used for Quenching. If the quench tank water is of poor quality (e.g. using process water with a higher percentage of contaminants), the regenerated carbon may adsorb contaminants at this stage, including both organic and inorganic substances.

As evidenced by ICP analysis, the quench water sample showed higher concentrations of inorganic contaminants. This significantly reduces the carbon’s activity, affecting its kinetic properties, gold adsorption capacity, and overall recovery rates. However, this issue does not occur in all gold processing operations.

Regeneration Issue

In this process, froth flotation utilizes organic reagents to recover gold concentrate. However, these reagents often carry over into the CIL process, contaminating the activated carbon and diminishing its gold adsorption efficiency. This indicates that the activated carbon regeneration process was not fully successful.

In this case, regeneration must be performed under more stringent conditions and at higher temperatures than usual because some reagents, particularly Potassium Amyl Xanthate (an organosulfur compound), bind very strongly to the carbon pores.

Particle Size Distribution
Particle Size Distribution

The sample had a high concentration of fine carbon which led to increased carbon loss and consequently, gold loss. The regenerated sample contained 36.5% fine carbon (% mass finer than 1.7 mm), which exceeds acceptable norms for efficient carbon circuits. To minimize gold loss, it’s recommended to keep fine carbon content below 10%, as fine carbon can pass through interstage screens and be discharged into tailings. This is the root cause.

Root Cause

Screw Feeder Issues

In this process, froth flotation utilizes organic reagents to recover gold concentrate. However, these reagents often carry over into the CIL process, contaminating the activated carbon and diminishing its gold adsorption efficiency. This indicates that the activated carbon regeneration process was not fully successful.

In this case, regeneration must be performed under more stringent conditions and at higher temperatures than usual because some reagents, particularly Potassium Amyl Xanthate (an organosulfur compound), bind very strongly to the carbon pores.

Screw Feeder Issues

In this process, froth flotation utilizes organic reagents to recover gold concentrate. However, these reagents often carry over into the CIL process, contaminating the activated carbon and diminishing its gold adsorption efficiency. This indicates that the activated carbon regeneration process was not fully successful.

In this case, regeneration must be performed under more stringent conditions and at higher temperatures than usual because some reagents, particularly Potassium Amyl Xanthate (an organosulfur compound), bind very strongly to the carbon pores.

Solutions

Maintenance of expected regenerated carbon activity
Maintenance of expected regenerated carbon activity

The sample had a high concentration of fine carbon which led to increased carbon loss and consequently, gold loss. The regenerated sample contained 36.5% fine carbon (% mass finer than 1.7 mm), which exceeds acceptable norms for efficient carbon circuits. To minimize gold loss, it’s recommended to keep fine carbon content below 10%, as fine carbon can pass through interstage screens and be discharged into tailings. This is the root cause.

Improvement :

As the mine acquired the appropriate kiln tube and increased the kiln temperatures, they managed to achieve activities greater than 90%

The sample had a high concentration of fine carbon which led to increased carbon loss and consequently, gold loss. The regenerated sample contained 36.5% fine carbon (% mass finer than 1.7 mm), which exceeds acceptable norms for efficient carbon circuits. To minimize gold loss, it’s recommended to keep fine carbon content below 10%, as fine carbon can pass through interstage screens and be discharged into tailings. This is the root cause.

Improvement :

As the mine acquired the appropriate kiln tube and increased the kiln temperatures, they managed to achieve activities greater than 90%

Improvements to Screw Feeder operations
Improvements to Screw Feeder operations

Immediate replacement of the worn screw feeder was recommended. The materials used should be mild steel or stainless steel, with a preference for stainless steel (SUS 316L) due to its superior resistance to corrosion and wear. To enhance control capabilities, it was suggested to implement variable frequency drives like the Techno Variable Driver – 1HP. Additionally, it is crucial to maintain the clearance below 2.00 mm, with a maximum allowance of 5.00 mm.

Improvement :

Following changes to the screw feeder, there was a significant reduction (40-50%) in fine carbon content. This improvement underscores the importance of continuous monitoring and adjustments to the feeder systems to maintain optimal performance.

Immediate replacement of the worn screw feeder was recommended. The materials used should be mild steel or stainless steel, with a preference for stainless steel (SUS 316L) due to its superior resistance to corrosion and wear. To enhance control capabilities, it was suggested to implement variable frequency drives like the Techno Variable Driver – 1HP. Additionally, it is crucial to maintain the clearance below 2.00 mm, with a maximum allowance of 5.00 mm.

Improvement :

Following changes to the screw feeder, there was a significant reduction (40-50%) in fine carbon content. This improvement underscores the importance of continuous monitoring and adjustments to the feeder systems to maintain optimal performance.

General Recommendations by Our Experts to Improve Performance & Efficiency
General Recommendations by Our Experts to Improve Performance & Efficiency

Improve Kiln

Parameters

Optimize kiln settings to achieve higher carbon activity levels and more efficient gold adsorption.

Optimize

Particle Size

Ensure that the carbon supplied adheres to the standard 6/12 mesh specification to reduce fines and enhance retention.

Enhance Screw

Feeder Design

Utilize stainless steel feeders with variable frequency drives and maintain appropriate clearance to minimize attrition and ensure consistent feed rates.

Regular

Maintenance

Have a thorough maintenance schedule to monitor and fix wear and tear and avoid damage from foreign materials.

Improve Kiln Parameters

Optimize kiln settings to achieve higher carbon activity levels and more efficient gold adsorption.

Optimize Particle Size

Ensure that the carbon supplied adheres to the standard 6/12 mesh specification to reduce fines and enhance retention.

Enhance Screw Feeder Design

Utilize stainless steel feeders with variable frequency drives and maintain appropriate clearance to minimize attrition and ensure consistent feed rates.

Regular Maintenance

Have a thorough maintenance schedule to monitor and fix wear and tear and avoid damage from foreign materials.